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The synthesis of a series of sodium mono-alkylamide maleate surfactants was described, and the surface activity properties of the surfactants were studied. The mono-alkylamide maleic acids were synthesized by amidation using primary aliphatic amine (lauryl, myristyl, cetyl) and maleic anhydride as starting material. They were structurally characterized by IR,1H-NMR and MS. The sodium mono-alkylamide maleate surfactants were prepared by neutralization of the precursor mono-alkylamide maleic acids with sodium hydroxide. They reduced the surface tension of water to 32– 34 mN × m–1at concentration levels of 10–4–10–3mol × L–1.
From Fu Han | Bao-cai Xu | Zhi-qiang Qu | Ya-wen Zhou | Gui-ju Zhang
(Received 19.10.2011; revised 10.12.2011)
Appeared in Tenside Surfactants Detergents 2012/04, Page 340-342
Direct link: http://www.tsd-journal.com/TS110202
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Synthesis and Properties of Sodium Mono-alkylamide Maleate Surfactants [145 KB]
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